METHODS
TEST CONDITIONS:
-Condition the samples at least 24 h at 20 ± 2 ºC and 65 ± 4% RH. The trial should be started within 3 min after conditioning.
-The tests will be carried out in a room free of air currents and protected from any parasitic radiation that could be recorded by the calorimeter. The temperature of the room between 15-35ºC and the calorimeter has to be cooled to room temperature ± 2 ºC before each test.
-Heat flux density:
- Low levels: 5kW/m² to 10 kW/m²
- Average levels: 20 kW/m² to 40 kW/m²
- High levels: 80 kW/m²
-Calibration of the radiant heat source prior to the test is essential.
METHOD A: A sample is fixed to a vertical frame by applying a voltage of 2 N and exposed to a set level of radiant heat for a set amount of time.
The radiant heat level is fixed by adjusting the distance between the sample and the thermal radiation source. After the exposure, the sample and its layers are examined to determine any visible changes.
Evaluation: After irradiation, the sample or individual layers of the multilayer assembly are inspected. Any changes (e.g., discoloration, fouling, ember, charring, breakage, melting, shrinking, sublimation, etc.) that are observed are noted for the sample or for each individual layer of the multilayer assembly.
METHOD B: A sample is attached to a vertical frame (sample holder) by applying a voltage of 2 N and exposed to a set level of radiant heat. The times needed to obtain a temperature increase in the calorimeter of 12 ºC and 24 ºC are determined and expressed as radiant heat transfer indices. The percentage thermal transmission factor is calculated from the increase in temperature, and is also noted in the report.
The times t12 and t24, expressed in seconds with a decimal place, are determined to obtain an increase in the calorimeter temperature of (12 ± 0.1) ºC or (24 ± 0.2) ºC, respectively. As required in the specific standard, the result of the difference between t24 and t 12 is calculated and recorded.
Evaluation:
-The transmitted heat flux density QC is determined in Kw/m2
-The thermal transmission factor TF (Q0)
-Radiant heat transfer index RHTI12 (Q0, time measurement t12, expressed in 0.1 s for the calorimeter temperature increase of 12 ±0.2 ºC
-Radiant heat transfer index RHTI24 (Q0), time measure t24 expressed in 0.1 s for the calorimeter temperature increase of 24 ±0.2 ºC
-The radiant heat transfer index, RHTI24-RHTI12 (Q0) for the incident heat flux density is determined RHTI24 minus RHTI12.